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Cantilever selection for measuring adhesion force

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Bruker Employee
David Durham posted on Mon, Jun 10 2013 3:24 PM

Hi,

We are trying to measure the adhesion force between 48 Mm silica beads and silica substrate , and based on the theoretical model the expected value of adhesion is around 10 micro N , so what is the proper type of cantilever should we use??? 

Thanks

 

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Answered (Verified) Verified Answer

Top 10 Contributor
280 Posts
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Bruker Employee
Verified by David Durham

You should choose a cantilever that is sensitive as possible, but does not cause the deflection measurement to saturate or become non-linear.  

The force is the spring constant times the deflection sensitivity times the detector voltage (F=K*Sd*V).  If we know K for a given probe type and we know the approximate Sd (this depends on probe type, head, microscope type, and laser spot position), we can calculate the approximate detector voltage.  For best linearity the detector voltage should be in the range -2V to +2V (the system can measure up to +/-12V, but it is less linear, so accuracy will usually be less).

For example, some ballpark numbers for the Multimode are:

F (nN)

K (N/m)

~Sd (nm/V)

V

Probe

10000

350

75

0.380952

DNISP-HS

10000

150

75

0.888889

DNISP

10000

150

30

2.222222

TAP525A

10000

48

50

4.166667

LTESPA

Based on that I'd start with a TAP525A probe and see how it works.

--Bede

 

All Replies

Top 10 Contributor
280 Posts
Points 6,221
Bruker Employee
Verified by David Durham

You should choose a cantilever that is sensitive as possible, but does not cause the deflection measurement to saturate or become non-linear.  

The force is the spring constant times the deflection sensitivity times the detector voltage (F=K*Sd*V).  If we know K for a given probe type and we know the approximate Sd (this depends on probe type, head, microscope type, and laser spot position), we can calculate the approximate detector voltage.  For best linearity the detector voltage should be in the range -2V to +2V (the system can measure up to +/-12V, but it is less linear, so accuracy will usually be less).

For example, some ballpark numbers for the Multimode are:

F (nN)

K (N/m)

~Sd (nm/V)

V

Probe

10000

350

75

0.380952

DNISP-HS

10000

150

75

0.888889

DNISP

10000

150

30

2.222222

TAP525A

10000

48

50

4.166667

LTESPA

Based on that I'd start with a TAP525A probe and see how it works.

--Bede

 

Top 25 Contributor
42 Posts
Points 485
Bruker Employee

Thanks Bede!

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Top 75 Contributor
11 Posts
Points 125
mariam replied on Tue, Jun 11 2013 4:22 PM

This may be a bit out of the topic but I would also like to inquire what suggestions you may have for measurements of elastic modulus for ceramic samples  with roughness of 0.4-2 microns..

Thank you

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Top 10 Contributor
280 Posts
Points 6,221
Bruker Employee

please see the response in your other thread: http://nanoscaleworld.bruker-axs.com/nanoscaleworld/forums/t/1445.aspx

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