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  • Re: Normal force calculation in fluid

    Thanks!!
    Posted to SPM Digest (Forum) by dave11420 on Wed, Apr 4 2012
  • Normal force calculation in fluid

    If I have a silicon substrate and I want to measure normal forces, I take the change in setpoint x the cantilever stiffness x the sensitivity from the force displacement (fd) curves. However, if I am scanning in a liquid (fluid cell) do I use the sensitivity from the fd curves from the liquid or the fd curves from the silicon substrate in air?
    Posted to SPM Digest (Forum) by dave11420 on Mon, Apr 2 2012
  • Re: thin film with gold and dodecane

    Alex, I would like to create a thin film on silica with glycerol and Au particles. The Au comes suspended in water. Since glycerol is soluble in water, I mix the two, diluting the glycerol down to anywhere between 2-5%. I either try dip coating or spin coating, but there doesn't seem to be any particles on the substrate. The Au particles tend to
    Posted to SPM Digest (Forum) by dave11420 on Wed, Dec 7 2011
  • thin film with gold and dodecane

    I'm trying to create a ~2-3 nm thick film with glycerol and gold nanoparticles(30 nm in dia.). The gold particles are in suspension in DI water. I've tried a 5% solution (diluted glycerol) and the DI and gold using a dip coating process with withdraw speed (0.75 mm/min). The film thickness is ~100-200 nm. Spin coating is even worse. Does anyone
    Posted to SPM Digest (Forum) by dave11420 on Tue, Nov 22 2011
  • Re: lateral signal drift

    Hi Stefan, I usually let it warm up for 1hr then start using it. I usually have TMR values around 300mv, eventually iy gets up to the 2V, stays there for abt 2-3mins and drifts back down again. I'm attaching a 50micron borosilicate ball to a 3N/m stifness cantilever. The shift goes up, then comes back down and repeats. Regards, Dave
    Posted to SPM Digest (Forum) by dave11420 on Mon, Aug 8 2011
  • lateral signal drift

    When using the afm (multi mode) in lateral force mode, I've noticed that after turning it on the TMR values are in the mV range after scanning for more than 2 hrs, it begins to drift and eventually reaches the voltage range (2-3V). Could this be due to the age of the afm? I believe that it is about 10 yrs old, and might need servicing. How reliable
    Posted to SPM Digest (Forum) by dave11420 on Mon, Aug 8 2011
  • Borosilicate ball on tip

    Has anyone tried attaching a borosilicate ball to a triangular cantilever (.58n/m stiffness) to take measurements (friction) on a substrate like silica (1,0,0). Even without the ball and a regular tip the vertical sum signal starts increasing in the positive direction before it actually engages. Also when scanning, increasing the set point causes the
    Posted to SPM Digest (Forum) by dave11420 on Mon, Aug 8 2011
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